The performance of engineered cementitious composites (ECCs) under coupled salt freezing and loaded conditions is important for its application on the transportation infrastructure. However, in most of the studies, the specimens were generally loaded prior to the freezing. The influence of sustained load was merely considered. To this end, four sustained deflection levels, i.e., 0%, 10%, 30% and 50% of the deflection at the ultimate flexural strength, and three salt concentrations (1%, 3% and 5%) were applied. Prior to the salt frost resistance test, the fluid absorption of ECC specimens under various conditions were measured. The changes in relative dynamic elastic modulus (RDEM) during the freeze–thaw cycles were captured. The depth and the content profile of free chloride were measured after the coupled sustained load and freezing and thawing cycles. It is shown that 3% NaCl solution leads to the largest deterioration in all cases. There is no visible flaking or damage occurring on the surface. The relationships between locally sustained flexural stress and RDEM loss and also locally sustained flexural stress and free chloride penetration depth were proposed and showed satisfactory results. It is concluded that when ECC is subjected to the FTCs under 1% de-ice salt solution, no depassivation of the steel is expected even under a large deflection level. In terms of 3% and 5% salt solution, the thickness of cover should be no less than 20 mm when a deflection level of 0.5 is applied.

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The mechanical performance of engineered cementitious composite (ECC) depends greatly on fiber orientation and distribution. In this paper, the effect of fiber orientation on ECC's mechanical properties was investigated using two different casting methods: a flow-induced casting was used to enhance the fiber orientation within ECC mixture and compared with the conventional casting. The fiber orientation was quantified using scanning electron microscope (SEM) and image processing. Mechanical tests on the specimens with various fiber orientations were performed. The failure processes of ECC specimens under compression and tensile tests were analyzed using digital image correlation (DIC) technique. The proposed flow-induced casting enhanced the fiber alignment in the flow direction. Consequently, ECC's mechanical properties were significantly improved with more finer cracks under uniaxial loading. In conclusion, the proposed flow-induced casting can be adopted as an effective approach to improve fiber bridging efficiency in ECC.@en

This paper presents a study on cracking characterization of engineered cementitious composites (ECC) under flexural cyclic load using digital image correlation (DIC) technique. Five stress levels, namely 0.65, 0.75, 0.8, 0.85 and 0.9 of the flexural strength, were applied. Strain map at the side surface was obtained by DIC and used to drive evolution of the midspan deflection, damage pattern, maximum crack width, number of cracks, and crack width distribution with respect to the normalized number of cycles. The stress level was found to have a significant influence on the cracking behavior of ECC under flexural cyclic load. Regardless of the applied stress level, most of the crack widths are in the range between 20 and 80 μm. In the end, a two-dimension Gauss function was used to correlate the crack width distribution with normalized number of cycle and shows satisfactory results.@en

Carbide residue activated blast furnace slag is a relatively new kind of eco-friendly construction materials. This work addresses the design of foamed lightweight concrete as road embankment material using such material. A statistical mixture design approach was adopted to assess the influence of each ingredient as well as the interaction between these on the spreadability and compressive strength and thus allowing mixture design. The fitted models were validated using analysis of variance, residual analysis and confirmed by the experiments. Afterwards, the proposed models were used to optimize the mixture. The mixture with the highest compressive strength and the maximum content of carbide residue that allows the mixture to meet the required properties were obtained, respectively.

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Engineered cementitious composites (ECCs) belong to a broad class of fibre-reinforced concrete. They incorporate synthetic polyvinyl alcohol (PVA) fibres, cement, fly ash and fine aggregates, and are designed to have a tensile strain capacity typically beyond 3%. This paper presents an investigation on the carbonation behaviour of engineered cementitious composites (ECCs) under coupled sustained flexural load and accelerated carbonation. The carbonation depth under a sustained stress level of 0, 0.075, 0.15, 0.3 and 0.6 relative to flexural strength was measured after 7, 14 and 28 days of accelerated carbonation. Thermogravimetric analysis, mercury intrusion porosimetry and microhardness measurements were carried out to show the coupled influence of sustained flexural load and accelerated carbonation on the changes of the mineral phases, porosity, pore size distribution and microhardness along the carbonation profile. A modified carbonation depth model that can be used to consider the coupled effect of flexural tensile stress and carbonation time was proposed. The results show that an exponential relationship can be observed between stress influence coefficient and flexural tensile stress level in the carbonation depth model of ECC, which is different when using plain concrete. Areas with a higher carbonation degree have greater microhardness, even under a large sustained load level, as the carbonation process refines the pore structure and the fibre bridges the crack effectively.

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In this study, the flexural strength and fatigue properties of interfacial transition zone (ITZ) were experimentally investigated at the micrometre length scale. The hardened cement paste cantilevers (150 × 150 × 750 μm³) attached to a quartzite aggregate surface were prepared and tested under the monotonic and cyclic load using a nanoindenter. The measured flexural strength of the ITZ (10.49–14.15 MPa) is found to be one order of magnitude higher than the macroscopic strength of ITZ reported in literature. On the other hand, the fatigue strength of the ITZ is lower than that of bulk cement paste at same length scale, measured previously by the authors. The microscopic mechanical interlocking and the electrostatic interaction between aggregate surface and hydration products are thought to contribute to the bond strength of ITZ. This study provides an experimental basis for the development of multiscale analysis of concrete subjected to both static and fatigue loading.

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This work presents a study of mechanical properties of foamed concrete at the meso-scale based on a combination of X-ray computed tomography (XCT) technique and a discrete lattice type fracture model. The microstructure of the foamed concrete with different densities was obtained by XCT technique and binarized as two-phase (pore/solid) materials. The parameters (e.g., porosity, pore diameter and spacing distribution) of foamed concrete air‐void structure were characterized. The virtual specimens were subjected to computational uniaxial compression, Brazilian splitting and three-point bending test to calculate strengths and elastic modulus. The mechanical properties of solid phase were derived from the recent outcome of micromechanical models. Two types of element input parameters were used to investigate the influence of the input parameters on the simulated results. The modelling results (strength value and fracture pattern) were compared with the experiments. It shows that, without further calibration, the lattice model can predict the mechanical strength and crack pattern with good accuracy. The fracture toughness KIC was derived using three-point bending strength and the average pore diameter. The results indicate that the presence of air-void structure increases the brittleness and reduces the fracture toughness of the foamed concrete.@en

This paper explores buildability quantification of randomly meshed 3D printed concrete objects by considering structural failure by elastic buckling. The newly proposed model considers the most relevant printing parameters, including time-dependent material behaviors, printing velocity, localized damage and influence of sequential printing process. The computational uniaxial compression tests were first conducted to calibrate age-dependent elastic modulus and yield stress. Subsequently, analyses of the 3D printing process of a free wall structure and a square layout were performed. The model can reproduce the asymmetry of buckling failure accurately and the predicted critical printing height is in excellent agreement with experimental data from the literature. It can be concluded the combined effect of material variability and non-uniform gravitational loading due to sequential printing process resulted in structural failure during 3D concrete printing. Using this model, printing parameters can be optimized and a suitable printing scheme can be devised to improve structure buildability.

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The resistance of cracked ECC against chloride ingress is mainly governed by the accumulated crack width of all the cracks rather than the maximum width of multiple cracks. However, most studies focus on the influence of a single fine crack@en

This paper presents a method to numerically investigate the microstructural effect on the creep behavior of cement paste at the microscale. The lattice fracture model is extended to consider local time-dependent deformations of calcium-silicate-hydrate phases in the cement paste by imposing local forces. The term “experimentally informed model” is used herein as the heterogeneous microstructures of hardened cement pastes were obtained by using the X-ray computed microtomography and directly implemented into the model. The mechanical and creep properties of different constituents at the resolution of 5 µm were inversely identified from the fracture and creep bending tests on cementitious microcantilever beams at the microscale. The model is then validated through the comparison with the testing results of cement pastes with different w/c ratios and microstructures. It is found that the developed model can successfully reproduce experimentally observed behaviors and be applied to explain the experimental results in detail. With the method presented in this paper, the relationship between the volume fractions of different components and the global creep behavior of cement paste can be established. The validation of the model performed at the microscale forms a basis for the multiscale analysis of concrete creep.

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The elastic modulus of corrosion product (E_cp) has been reported with significant variations in the literature. This study aims to investigate the E_cp of naturally-generated chloride-induced corrosion products formed in different concrete mixes. Microstructural characterization was conducted through nano-indentation, electron microscopy and Raman spectroscopy. The corrosion products were mainly composed of a goethite matrix with portions of maghemite, independently of the concrete composition. Microscopic analysis suggest that layers of corrosion products grow at different times and under different physico-chemical conditions. Our measurements showed that E_cp varied between 80−100 GPa, which can be suggested for numerical models of corrosion induced cracking.

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An important input parameter for numerical models that simulate cracking of the concrete cover due to reinforcement corrosion is the Elastic modulus of corrosion product (Ecp). Despite its relevance, Ecp is subject of significant variations according to the values reported in the literature, which vary from less than 100 MPa up to 360 GPa. Furthermore, Ecp values proposed in most of the present literature are representative of the corrosion product generated by anodic accelerated corrosion or extracted from the steel/concrete interface (SCI), which might differ from that formed in real corroding structures. Therefore, this study aims to investigate the Elastic modulus of naturally-generated corrosion product present at the SCI through nano-indentation conducted on six reinforced concrete polished sections. The polished sections were obtained from six 20-year-old reinforced concrete prisms cast with different cement type (CEM I, CEM II/B-V, CEM III/B, CEM V/A), same water/binder ratio (0.55) and which were previously exposed to NaCl solution wet/dry cycles. This study revealed that the range of Ecp did not considerably vary between corrosion products formed in different concrete mixes. However, corrosion product was microscopically found to consist of overlapping bands with different Ecp, varying for up to around 70 GPa between each other. Through Environmental Scanning-Electron Microscopy (ESEM) and Energy Dispersive Xray Spectrometry (EDS) analysis of the indented locations, it was found that Ecp is highly dependent on the presence of interfacial cracks and inversely proportional to the concentration of Si and Ca, representative for corrosion product mixed with the surrounding concrete. Furthermore, higher concentration of Fe leads to higher Ecp. Based on this study, an average range of values for Ecp between 80-100 GPa can be suggested for use in numerical models for corrosion induced cracking, regardless of cement type of the structure under investigation.@en

Clay brick is one of the major components of demolition waste, which is generally landfilled. Effective and new uses of recycled clay brick may provide sustainability benefits in terms of landfill reduction. Therefore, this research aims at applying Recycled fine clay brick aggregates (RFCBA) with sizes from 0.075 mm–4.75 mm to prepare Self-compacting concrete (SCC). The effects of RFCBA on fresh and hardened properties of SCC were investigated. Saturated surface dry RFCBA was used to replace Natural fine aggregate (NFA) with the percentage of 25%, 50%, 75% and 100%, respectively, in making the SCC mixes. Although experimental results showed that the flowability, passing ability, and segregation resistance of SCC containing RFCBA (RFCBA-SCC) decreased with the increasing RFCBA content, these properties still satisfy the criteria of SCC. The compressive strength, splitting strength, flexural strength, and elastic modulus of the RFCBA-SCC mixes decreased with an increase of RFCBA content. Due to their porous nature, recycled fine clay brick aggregates may also be a source of additional water for internal curing. The internal curing effect was confirmed by the mercury intrusion porosimetry, X-ray diffraction, and thermogravimetric analysis measurements. Moreover, a significant autogenous shrinkage reduction of SCC is achieved by using the RFCBA due to the release of additional water pre-stored in the RFCBA. Therefore, it can be concluded that the addition of RFCBA to SCC mixtures can provide additional practical benefits in the hardened state.@en

This study presents an experimental investigation of fatigue properties of cement paste at the microscale. A strong size dependence is found for the flexural fatigue life of the cement paste specimen. Microscopic observations on the fractured surfaces suggest that there is a higher density of nano-scale cracks generated during the fatigue loading compared to the static fracture. However, the fatigue damage evolution is found to be very slow and small even under high stress levels. The development of residual deformation for cement paste can be explained by the combined effects of viscoelastic deformation and fatigue cracking growth.

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In this study, a numerical model using a 2D lattice network is developed to investigate the fatigue behaviour of cement paste at the microscale. Images of 2D microstructures of cement pastes obtained from XCT tests are used as inputs and mapped to the lattice model. Different local mechanical and fatigue properties are assigned to different phases of the cement paste. A cyclic constitutive law is proposed for considering the fatigue damage evolution. Fatigue experiments performed at the same length scale are used to calibrate and validate the model. The proposed model can reproduce well the flexural fatigue experimental results, in terms of S-N curve, stiffness degradation and residual deformation. The validated model is then used to predict the uniaxial tensile fatigue fracture of cement paste. The effects of microstructure and stress level on the fatigue fracture are studied using the proposed model. This model forms a basis for the multiscale analysis of concrete fatigue.

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This study proposes an experimental method for studying the short-term creep behaviour of cement paste at micro-scale. The micro-bending tests on miniaturized cantilever beams were used to characterize the viscoelastic properties of cement paste. The effects of w/b ratio, the type of binder and the stress level on the microscopic creep behaviour were investigated. It is found that the short-term creep of cement paste at microscale can be satisfactorily described by a power-law function. A linear viscoelastic behaviour has been observed in different cementitious systems at the microscale with the stress level up to 67.9%. When compared with the creep results in microindentation tests and conventional macroscopic tests, the obtained creep compliance function in this study is found to be both qualitatively and quantitatively representative of the macroscopic results. This experimental study underlines the importance of microstructural effect on the creep behaviours of cementitious materials at microscale.

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The lattice fracture model is a discrete model that can simulate the fracture process of cementitious materials. In this work, the Delft lattice fracture model is reviewed and utilized for fracture analysis. First, a systematic calibration procedure that relies on the combination of two uniaxial tensile tests is proposed to determine the input parameters of lattice elements—tensile strength, compressive strength and elastic modulus. The procedure is then validated by simulating concrete fracture under complex loading and boundary conditions: Uniaxial compression, three-point bending, tensile splitting, and double-edge-notch beam shear. Simulation results are compared to experimental findings in all cases. The focus of this publication is therefore not only on summarizing existing knowledge and showing the capabilities of the lattice fracture model; but also to fill in an important gap in the field of lattice modeling of concrete fracture; namely, to provide a recommendation for a systematic model calibration using experimental data. Through this research, numerical analyses are performed to fully understand the failure mechanisms of cementitious materials under various loading and boundary conditions. While the model presented herein does not aim to completely reproduce the load-displacement curves, and due to its simplicity results in relatively brittle post-peak behavior, possible solutions for this issue are also discussed in this work.@en