The steel–concrete interface (SCI) is known to play a major role in corrosion of steel in concrete, but a fundamental understanding is still lacking. One reason is that concrete’s opacity complicates the study of internal processes. Here, we report on the application of bimodal X-ray and neutron microtomography as in-situ imaging techniques to elucidate the mechanism of steel corrosion in concrete. The study demonstrates that the segmentation of the specimen components of relevance—steel, cementitious matrix, aggregates, voids, corrosion products—obtained through bimodal X-ray and neutron imaging is more reliable than that based on the results of each of the two techniques separately. Further, we suggest the combination of tomographic in-situ imaging with ex-situ SEM analysis of targeted sections, selected based on the segmented tomograms. These in-situ and ex-situ characterization techniques were applied to study localized corrosion in a very early stage under laboratory chloride-exposure conditions, using reinforced concrete cores retrieved from a concrete bridge. Several interesting observations were made. First, the acquired images revealed the formation of several corrosion sites close to each other. Second, the morphology of the corrosion pits was relatively shallow. Finally, only about half of the total 31 corrosion initiation spots were in close proximity to interfacial macroscopic air voids, and > 90% of the more than 160 interfacial macroscopic air voids were free from corrosion. The findings have implications for the mechanistic understanding of corrosion of steel in concrete and suggest that multimodal in-situ imaging is a valuable technique for further related studies.

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The technique of neutron tomography has, after 350 years, enabled a first look inside the iconic single-lens microscopes of Antoni van Leeuwenhoek. Van Leeuwenhoek's 17th-century discovery of "animalcules"marks the birth of microbiology. His skillfully self-produced microscope lenses remained unsurpassed for over 150 years. Neutron tomography now enabled us to reveal the lens types Van Leeuwenhoek used. We argue that Van Leeuwenhoek's instruments incorporate some innovations that testify to an awareness of concurrent developments. In particular, our analysis shows that for making his best-performing microscopes, Van Leeuwenhoek deployed a lens-making procedure popularized in 1678 by Robert Hooke. This is notable, as Hooke always wanted to find the secret of Van Leeuwenhoek's lenses, but never managed to do so. Therefore, Van Leeuwenhoek was far from the isolated scholar he is often claimed to be; rather, his secrecy about his lenses was motivated by an attempt to conceal his indebtedness to Hooke.

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A rare find of a high-status 17th century oval box, retrieved from a shipwreck, provided a unique opportunity to research the construction and finishing layers of an object that is untouched for 350 years. This case study was used to demonstrate the extent of data that can be gained from analytical techniques prior to conservation. The amalgam-gilt brass object was studied by optical and electron microscopy, X-radiography, micro-computed X-ray tomography, neutron tomography, X-ray fluorescence, X-ray diffraction, Rutherford backscattering spectrometry, proton-induced X-ray emission and gas chromatography. The results have led to a characterisation of the manufacturing methods used on the box and to a better understanding of the practicality of modern analytical methods and techniques in (maritime) archaeological research.

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A neutron imaging detector based on neutron-sensitive microchannel plates (mcps) was constructed and tested at beamlines of thermal and cold neutrons. The mcps are made of a glass mixture containing 10B and natural Gd, which makes the bulk of the mcp an efficient neutron converter. Contrary to the neutron-sensitive scintillator screens normally used in neutron imaging, spatial resolution is not traded off with detection efficiency. While the best neutron imaging scintillators have a detection efficiency around a percent, a detection efficiency of around 50% for thermal neutrons and 70% for cold neutrons has been demonstrated with these mcps earlier. Our tests show a performance similar to conventional neutron imaging detectors, apart from the orders of magnitude better sensitivity. We demonstrate a spatial resolution better than 150 Um. The sensitivity of this detector allows fast tomography and neutron video recording, and will make smaller reactor sites and even portable sources suitable for neutron imaging.@en

We present a comprehensive structural characterization of two different highly pure nuclear graphites that compasses all relevant length scales from nanometers to sub-mm. This has been achieved by combining several experiments and neutron techniques: Small Angle Neutron Scattering (SANS), high-resolution Spin Echo SANS (SESANS) and neutron imaging. In this way it is possible to probe an extraordinary broad range of 6 orders of magnitude in length from microscopic to macroscopic length scales. The results reveal a fractal structure that extends from ∼0.6 nm to 0.6 mm and has surface and mass fractal dimensions both very close to 2.5, a value found for percolating clusters and fractured ranked surfaces in 3D.@en