Micro/nanoscale additive manufacturing provides a powerful tool for advanced materials and structures with complex and precise features. For instance, the feature resolution of two-photon polymerization (2PP) can reach 200 nm. At this scale, materials properties can change, and the influence of the size effect cannot be ignored. Therefore, it is necessary to assess changes in the material mechanical properties considering size effects. In this work, several micrometric polymeric specimens are printed via 2PP, and their mechanical properties are assessed using compression tests. Detailed printing and testing procedures and the effects of parameter settings are provided. The experimental results show that the changes in the microstructures size have a direct effect on Young s modulus. In particular, a large surface-volume ratio results in a higher Young s modulus. In other words, the smaller the structure size, the higher the stiffness. The reported findings play a significant role in the development of fabrication strategies for polymeric microstructures where high stiffness accuracy is fundamental.

The phase transformations, microstructure and properties of two Medium-Mn processed via quenching and partitioning steels were compared in this contribution and a new strategy for controlling mechanical properties by introducing and controlling cold-worked ferrite prior to heat treatment is proposed. It was found that during heating, the recovery and recrystallization of cold-worked ferrite compete with austenitization, thereby inhibiting the coarsening of austenite. The cold-worked ferrite interface will significantly delay the austenitization kinetics during the partitioning local equilibrium stage compared to martensite. These results lead to a diverse parent austenite, as well as a refined martensite substructure. As a result, the randomly distributed variants increase the number of effective grain boundaries, thus enhancing yield strength. The intercritical annealing process at a temperature of 860 °C resulted in the formation of fresh martensite-retained austenite (M/RA) constituents exhibiting a remarkably fine (<2 μm) and uniform grain morphology. Such microstructure yielded substantial improvement in both the strength and ductility of the steel. The proposed treatment led to excellent elongation (24%) at fracture, combined with very high ultimate tensile strength and yield strength of 1345 MPa and 1163 MPa, respectively, of the steel, resulting in a product of strength and elongation that exceed 32 GPa%.