The importance of physico-chemical processes at the particle scale for the engineering scale behaviour of fine-grained geomaterials is undisputed. Yet, despite great advances in the discipline, experimental evidence that fully resolves the clay micromechanics i.e. linking the evolving microstructure and interparticle actions under loading, is lacking. This paper will discuss the challenges ahead in quantifying the evolving kinematics and interparticle interactions of finegrained geomaterials. As such, the current limitations, and the potential opportunities of experimental methodologies for manipulating, monitoring and (post-mortem) analysing fine-grained materials at the particle scale will be discussed. In addition to the need of integrating multiple experimental techniques that span several length scales and modalities, the critical role of advanced data reduction and analysis is highlighted, as required for a measurement as opposed to qualitative observation. Throughout the paper, the link between experimental clay micromechanics and modelling will be discussed.@en

Cement-bentonite cut-off walls are commonly employed in geoenvironmental applications to limit ground water flow and pollutant transport. The wide diffusion of this artificial material in the current practice is not only due to its low permeability, but also to its simplicity of use. In this paper, experimental evidences about the role of curing on the hydro-mechanical behaviour of cement-bentonite mixtures are presented. Different curing times and curing conditions (representative for either water saturated or hydrocarbon polluted soils) have been considered, and their effects on both hydraulic conductivity and mechanical response in oedometer and triaxial conditions have been assessed. A unified hydro-mechanical framework, accounting for the changes of material fabric occurring with curing time and environment, is formulated. The hydraulic conductivity is very well predicted by a Kozeny-Carman like equation, whereas the mechanical behaviour is finely reproduced via an enhanced elastic–plastic constitutive model.

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Soils used in earth construction projects are mostly unsaturated, and they undergo frequent drying–wetting cycles (repeated hydraulic loads) due to changes in climatic conditions or variations of the ground water level, particularly at shallow depths. After compaction, changes in water content can significantly influence the hydromechanical response of the construction material, which therefore must be assessed for repeated hydraulic loads. This research investigates the effect of such loads on the microstructure and hydraulic behaviour of a silty soil, typically used in the construction of embankments and dykes, with the aim of providing a better understanding of the consequences of drying–wetting cycles on the response of the material over time. Experimental tests were performed to study the impact of drying–wetting cycles on the water retention, hydraulic conductivity, and fabric of compacted specimens. Fabric changes are documented to take place even without significant volumetric strains, promoting an irreversible increase in the hydraulic conductivity and a reduction in the capacity to retain water compared to the as-compacted soil. The fabric changes are interpreted and quantified by means of a hydromechanical model, which accounts for the evolving pore-size distribution at different structural levels. The proposed model reproduces quite well the microstructural observations, together with the evolution of the water retention behaviour and hydraulic conductivity.

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The paper focuses on the hydromechanical behaviour of an unsaturated compacted clayey silt, accounting for fabric changes induced by drying–wetting cycles occurring at low stress levels. The response along isotropic compression and triaxial compression (shear) at constant water content was investigated by laboratory tests on both as-compacted and dried–wetted samples. Compaction induces a microstructural porosity pertinent to clay peds and a macrostructural porosity external to the peds. Drying–wetting cycles decrease the microporosity and increase the macroporosity, which reduces the water retention capacity, increases the compressibility, and promotes higher peak strengths with more brittle behaviour during triaxial compression. A coupled double-porosity elastic–plastic model was formulated to simulate the experimental results. A nonassociated flow rule was defined for the macrostructure, modifying a stress–dilatancy relationship for saturated granular soils to account for the increase in dilatancy with suction observed in the experiments. The average skeleton stress and suction were adopted as stress variables. As correctly predicted by the model, the shear strength at critical state is not significantly influenced by the degree of saturation or by the hydraulic history. On the contrary, the higher peak strength, brittleness, and dilatancy of the dried–wetted samples are mostly explained by their reduced water-retention capacity.@en

A comprehensive description of the water retention behaviour of unsaturated soils requires accounting for the hysteresis caused by hydraulic and mechanical wetting-drying cycles. A hysteretic water retention model is proposed by introducing the liquid-solid contact angle to account for the dependency of the response on non-monotonic changes in suction and void ratio. The proposed model reproduces main drying and wetting surfaces and also nonlinear scanning curves during hydraulic or mechanical loading. Experimental tests and numerical simulations were carried out to study the water retention behaviour of a clayey silt. The model simulations captured the experimental results well.

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