Optical turbidity and acoustic sensors have been widely used in laboratory experiments and field studies to investigate suspended particulate matter concentration over the last four decades. Both methods face a serious challenge as laboratory and in-situ calibrations are usually required. Furthermore, in coastal and estuarine environments, the coexistence of mud and sand often results in multimodal particle size distributions, amplifying erroneous measurements. This paper proposes a new approach of combining a pair of optical turbidity-acoustic sensors to estimate the total concentration and sediment composition of a mud/sand mixture in an efficient way without an extensive calibration. More specifically, we first carried out a set of 54 bimodal size regime experiments to derive empirical functions of optical-acoustic signals, concentrations, and mud/sand fractions. The functionalities of these relationships were then tested and validated using more complex multimodal size regime experiments over 30 optical-acoustic pairs of 5 wavelengths (420, 532, 620, 700, 852 nm) and six frequencies (0.5, 1, 2, 4, 6, 8 MHz). In the range of our data, without prior knowledge of particle size distribution, combinations between optical wavelengths 620–700 nm and acoustic frequencies 4–6 MHz predict mud/sand fraction and total concentration with the variation <10% for the former and <15% for the later. The results also suggest that acoustic-acoustic signals could be combined to produce meaningful information regarding concentration and mud/sand fraction, while no useful knowledge could be extracted from a combination of optical-optical pairs. This approach therefore enables the robust estimation of suspended sediment concentration and composition, which is particularly practical in cases where calibration data is insufficient.

The Mekong river is one of the largest rivers in the world, which flows through six countries of Southeast Asia (China, Myanmar, Laos, Thailand, Cambodia and Vietnam). Its hydro-sedimentary regime is changing rapidly, as a consequence of a regional shift of land use (agriculture, road, etc.), damming, sand mining and climate changes, among others. This study assesses the behavior of particles transported in suspension in the Lower Mekong River (LMR), along approximately 1700 km from fluvial to estuarine environments. Suspended sediment properties were estimated, simultaneously with hydrodynamic conditions, during three field campaigns. In addition, further investigations were performed in the laboratory to assess the structures of particles (flocculated or not), their capacity to flocculate (and the impacts on siltation), under a wide range of sediment concentration (20–30,000 mg.L⁻¹). This study confirms that suspended sediment transported in the LMR are predominantly (75% by volume) flocculi (or freshly eroded soils aggregates), with median aggregated particle size in the range 10–20 μm and median settling velocity of the order of 0.01–0.1 mm s⁻¹. These flocculi are robust under the hydrodynamic conditions (turbulence and suspended sediment concentration – SSC) existing in the LMR. Laboratory investigations reveal the existence of a threshold sediment concentration (400 mg.L⁻¹), beyond which flocculation and sedimentation increase of orders of magnitudes. Thus, concentration that exceeds this threshold might promote the formation of so-called fluid mud layers. Because of the nonlinear response of flocculation and sedimentation with SSC and considering the ongoing changes at a regional scale in the LMR, higher occurrence of fluid mud layers in the fluvial upstream waterbodies might be anticipated, and a lower occurrence in estuaries and alongshore where the concentration decrease. The geomorphology could be impacted, with an over-siltation in dams and an exacerbated erosion of the muddy-mangrove coast.