Polymer composite laminates have established themselves as essential materials across a wide type of industrial fields because of their specific mechanical properties such as high strength and low weight. Among the main issues they face is susceptibility to delamination damage. This comprehensive review paper investigates various damage mechanisms and associated phenomena that obvious during delamination within polymer composite laminates. Delamination can primarily arise in Mode I, Mode II and mixed Mode I &II loading scenarios. Notably, the damage features can vary significantly between these conditions. This paper aims to characterize and identify delamination-dominated damage features by conducting a comprehensive examination of the parameters that influence these features, all based on an extensive literature review and utilizing fractography analysis. The findings of this review illustrate the valuable insights that can be obtained from delamination fracture surfaces through the utilization of fractography images and the examination of damage features. For instance, it is possible to recognize details such as determining of global crack growth direction, calculating the rate of fatigue crack growth, and anticipating of strain energy released rate. This deeper understanding aids in pinpointing the key factors contributing to delamination damage. It could offer valuable insights for designing composites resistant to delamination. Additionally, it may assist in determining the underlying causes of catastrophic failures in tragic events.

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The study considers the delamination resistance of carbon/epoxy laminates modified with Thermoplastic Nanoparticles of Polysulfone (TNPs). A new electrospinning nanofiber technique was utilized to convert polysulfone polymer into nanoparticles and uniformly disperse them within the resin. Fracture toughness was evaluated under loading modes I and II. In mode I, the toughness (GIC) increased significantly from 170 to 328 J/m² with TNPs incorporation. However, mode II showed minimal change, with GIIC values of 955 J/m² for virgin and 950 J/m² for TNPs-modified specimens. Scanning Electron Microscopy (SEM) was employed to depict the influence of TNPs on damage characteristics and crack propagation patterns. In mode I, crack deviation enhanced toughness as TNPs bypassed the PSU, while in mode II, cracks propagated through TNPs, resulting in particle smearing on the epoxy surface. This highlights TNPs' potential to modify the fracture toughness in mode I loading, but their effect is constrained in mode II loading scenarios.@en

In this study, the fatigue properties of carbon fiber-reinforced polymer (CFRP) composite laminates were investigated, specifically focusing on the incorporation of 100-µm polysulfone (PSU) nanofibers as an interleaving material. The PSU nanofibers were produced using the electrospinning technique. Both quasi-static and fatigue tests were conducted on both the reference specimens and the modified specimens to evaluate their mode-I performance. The results revealed an 85% increase in fracture toughness (G_IC) under quasi-static testing. The fatigue plots revealed a noteworthy reduction in the fatigue crack growth rate (da/dN) for the modified specimens due to new toughening mechanisms. Scanning electron microscopy (SEM) demonstrated that, the PSU nanofiber became melted and distributed in the interface, leading to phase separation and a sea-island structure. The presence of PSU microspheres caused crack deflection during delamination, which resulted in increased fracture and fatigue resistance.

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The aim of this study was to find the correlation between failure modes and acoustic emission (AE) events in a comprehensive range of thin-ply pseudo-ductile hybrid composite laminates when loaded under uniaxial tension. The investigated hybrid laminates were Unidirectional (UD), Quasi-Isotropic (QI) and open-hole QI configurations composed of S-glass and several thin carbon prepregs. The laminates exhibited stress-strain responses that follow the elastic-yielding-hardening pattern commonly observed in ductile metals. The laminates experienced different sizes of gradual failure modes of carbon ply fragmentation and dispersed delamination. To analyze the correlation between these failure modes and AE signals, a multivariable clustering method was employed using Gaussian mixture model. The clustering results and visual observations were used to determine two AE clusters, corresponding to fragmentation and delamination modes, with high amplitude, energy, and duration signals linked to fragmentation. In contrast to the common belief, there was no correlation between the high frequency signals and the carbon fibre fragmentation. The multivariable AE analysis was able to identify fibre fracture and delamination and their sequence. However, the quantitative assessment of these failure modes was influenced by the nature of failure that depends on various factors, such as stacking sequence, material properties, energy release rate, and geometry.@en